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. 2000 Dec:56 (Pt 12):1490-1.
doi: 10.1107/s0108270100012725.

4-Methyl-N-

S Banerjee  1 , AK Mukherjee, B Nandi, NG Kundu, M Helliwell
Affiliations

4-Methyl-N-

S Banerjee et al. Acta Crystallogr C. 2000 Dec.

Abstract

The title compound, C(20)H(19)NO(2)S(2), is formed by a palladium-copper-catalyzed reaction between 4-methyl-N-[2-(prop-2-ynylsulfanyl)phenyl]benzenesulfonamide and p-iodotoluene. The molecules contain three essentially planar parts, namely an aminothiophenol moiety (A), a toluenesulfone moiety excluding the oxo ligands (B) and a tolyl group (C), approximately orthogonal to each other; the dihedral angles A/B, A/C and B/C are 111.6 (1), 89.3 (1) and 101.4 (1) degrees, respectively. Intermolecular N-H.O hydrogen bonds link the molecules into infinite one-dimensional chains.

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