Atomic absorption spectrophotometric determination of 4-hydroxy-3-nitrobenzenearsonic acid (roxarsone) in premixes
- PMID: 1158837
Atomic absorption spectrophotometric determination of 4-hydroxy-3-nitrobenzenearsonic acid (roxarsone) in premixes
Abstract
Roxarsone (4-hydroxy-3-nitrobenzenearsonic acid) is extracted from the premix with aqueous 1% ammonium carbonate. The extract is filtered, diluted, and analyzed by atomic absorption spectrophotometry, using an air-acetylene flame and an arsenic electrodeless discharge lamp. The instrument response of the sample is compared to that of a standard solution of arsenic trioxide. Recoveries range from 99.7. to 100.4% and coefficients of variation range from 0.35 to 0.63%.
Similar articles
-
Graphite furnace atomic absorption spectrophotometric determination of 4-hydroxy-3-nitrobenzenearsonic acid, other organic arsenicals, and inorganic arsenic in finished animal feed.J Assoc Off Anal Chem. 1982 May;65(3):711-9. J Assoc Off Anal Chem. 1982. PMID: 7096254
-
Spectrophotometric determination of roxarsone in animal feeds.J Assoc Off Anal Chem. 1971 Jan;54(1):80-5. J Assoc Off Anal Chem. 1971. PMID: 5170701 No abstract available.
-
Atomic absorption spectrophotometric determination of dibutyltin dilaurate in finished feeds: collaborative study.J Assoc Off Anal Chem. 1977 Sep;60(5):1054-8. J Assoc Off Anal Chem. 1977. PMID: 893325
-
Determination of Roxarsone in feeds using solid phase extraction and liquid chromatography with ultraviolet detection.J AOAC Int. 1993 Sep-Oct;76(5):956-61. J AOAC Int. 1993. PMID: 8241824
-
Determination of arsenic and arsenicals in foods and other biological materials.Residue Rev. 1977;68:123-49. doi: 10.1007/978-1-4612-6355-5_5. Residue Rev. 1977. PMID: 337434 Review. No abstract available.