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. 2003 Apr 17;5(8):1301-3.
doi: 10.1021/ol034228d.

Synthesis of a tricyclic mescaline analogue by catalytic C-H bond activation

Kateri A Ahrendt  1 , Robert G Bergman, Jonathan A Ellman
Affiliations

Synthesis of a tricyclic mescaline analogue by catalytic C-H bond activation

Kateri A Ahrendt et al. Org Lett. .

Abstract

[reaction: see text] A tetrahydrobis(benzofuran) mescaline analogue has been prepared in six steps and 38% overall yield from (4'-O-methyl)methyl gallate. The key step in this synthesis is a tandem cyclization reaction via directed C[bond]H activation followed by olefin insertion.

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