doi: 10.1107/S0909049505015414.
Epub 2005 Jun 15.
Application notes on the use of softer X-rays for anomalous powder diffraction
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- PMID: 15968118
- DOI: 10.1107/S0909049505015414
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Application notes on the use of softer X-rays for anomalous powder diffraction
J Synchrotron Radiat.
2005 Jul.
Free article
Abstract
An in-vacuum diffractometer has been modified to collect powder diffraction data from a sample of promazine hydrochloride. Strong anomalous contrast has been observed at, or close to, the sulphur edge. Based on the data collected, a bespoke diffractometer has been designed that, together with minor changes to the geometry of the experiment, will enable the routine collection of powder data at absorption edges below 5.5 keV.
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