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. 2006 Aug 18;71(17):6644-7.
doi: 10.1021/jo0608117.

Incorporation of 2,6-di(4,4'-dipyridyl)-9-thiabicyclo[3.3.1]nonane into discrete 2D supramolecules via coordination-driven self-assembly

Hai-Bo Yang  1 , Neeladri Das, Feihe Huang, Adam M Hawkridge, David D Díaz, Atta M Arif, M G Finn, David C Muddiman, Peter J Stang
Affiliations

Incorporation of 2,6-di(4,4'-dipyridyl)-9-thiabicyclo[3.3.1]nonane into discrete 2D supramolecules via coordination-driven self-assembly

Hai-Bo Yang et al. J Org Chem. .

Abstract

The synthesis and characterization of three new supramolecular complexes 6-8 (a rhomboid and two hexagons) via coordination-driven self-assembly are reported in excellent yields (>90%). These assemblies have 2,6-di(4,4'-dipyridyl)-9-thiabicyclo[3.3.1]nonane 2 as the bridging tecton. All assemblies were characterized by multinuclear NMR (1H and 31P), mass spectrometry (ESI-MS and ESI-FT-ICR), and elemental analysis. The X-ray structure of the 120 degrees tecton 2 is also discussed.

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