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. 2006 Dec 27;128(51):16440-1.
doi: 10.1021/ja0670254.

The total synthesis of (+/-)-11-O-debenzoyltashironin

Silas P Cook  1 , Alessandra Polara, Samuel J Danishefsky
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The total synthesis of (+/-)-11-O-debenzoyltashironin

Silas P Cook et al. J Am Chem Soc. .

Abstract

The total synthesis of the putative non-peptidyl neurotrophic factor 11-O-debenzoyltashironin has been accomplished. The key transformation involves a biomimetic oxidative dearomatization/transannular Diels-Alder sequence that closes the tetracyclic carbon skeleton present in the natural product.

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