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. 2007 Jan 21;5(2):229-32.
doi: 10.1039/b616582f. Epub 2006 Dec 5.

Acyl palladium species in synthesis: single-step synthesis of alpha,beta-unsaturated ketones from acid chlorides

Russell J Cox  1 , Andrew S Evitt
Affiliations

Acyl palladium species in synthesis: single-step synthesis of alpha,beta-unsaturated ketones from acid chlorides

Russell J Cox et al. Org Biomol Chem. .

Abstract

Conditions are reported for the facile, one-pot synthesis of alpha,beta-unsaturated ketones via the palladium-catalysed cross-coupling of acyl chlorides with hydrozirconated acetylenes, and its use in the 2-step synthesis of D-5-O-benzyl deoxyxylulose.

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