Skip to main page content
U.S. flag

An official website of the United States government

Dot gov

The .gov means it’s official.
Federal government websites often end in .gov or .mil. Before sharing sensitive information, make sure you’re on a federal government site.

Https

The site is secure.
The https:// ensures that you are connecting to the official website and that any information you provide is encrypted and transmitted securely.

Access keys NCBI Homepage MyNCBI Homepage Main Content Main Navigation
. 2008 Feb 21;10(4):533-6.
doi: 10.1021/ol702718z. Epub 2008 Jan 23.

Spurring radical reactions of organic halides with tin hydride and TTMSS using microreactors

Takahide Fukuyama  1 , Masahide Kobayashi, Md Taifur Rahman, Naoya Kamata, Ilhyong Ryu
Affiliations

Spurring radical reactions of organic halides with tin hydride and TTMSS using microreactors

Takahide Fukuyama et al. Org Lett. .

Abstract

Tributyltin hydride-mediated radical reactions of organic halides were successfully carried out in a continuous flow system using a microreactor. The reactions proceeded within a very short period of time, coupled with quickly decomposing radical initiators such as V-65 and V-70. The continuous flow reaction system was applied to gram scale synthesis of a key intermediate for furofuran lignans.

PubMed Disclaimer

LinkOut - more resources