Wettability and bonding of self-etching dental adhesives. Influence of the smear layer

Abstract

Objectives: To evaluate dentin wettability and bonding of self-etching and total-etch adhesives on smear layer-covered and smear layer-free dentin.

Methods: Three self-etching adhesives (Clearfil SE Bond, AdheSE and Xeno III) and one total-etch adhesive (SingleBond) were evaluated. The substrates were mid coronal smear layer-covered and smear layer-free dentin. Dentin wettability by resins was studied from contact angle measurement using sessile drop method and Axisymmetric Drop Shape Analysis (ADSA). Shear-bond strength was evaluated using a push-out technique (ad hoc design). Data were analysed with two-way ANOVA and Tukey's test.

Results: Similar values of dentin wettability were obtained for all adhesives tested regardless the presence of smear layer. Even though, Xeno III and AdheSE exhibited slightly lower wettability (higher contact angles values) on smear layer-free dentin. Likewise, the presence of smear layer did not affect the shear-bond strength. Total-etch adhesive obtained higher shear-bond strength than self-etching adhesives, which obtained similar values.

Significance: Wettability is similar between self-etching and total-etch adhesives. The smear layer affects slightly the wettability of self-etching adhesives. Shear-bond strength is not sensitive to the smear layer presence. Total-etch adhesion is stronger than self-etching adhesion. There is no clear relationship between wettability and bond strength.