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. 2008 May 14:(18):2152-4.
doi: 10.1039/b801537f. Epub 2008 Apr 2.

Clean and efficient synthesis of O-silylcarbamates and ureas in supercritical carbon dioxide

Matthew J Fuchter  1 , Catherine J Smith, Melanie W S Tsang, Alistair Boyer, Simon Saubern, John H Ryan, Andrew B Holmes
Affiliations

Clean and efficient synthesis of O-silylcarbamates and ureas in supercritical carbon dioxide

Matthew J Fuchter et al. Chem Commun (Camb). .

Abstract

The synthesis of a family of O-silylcarbamates from the corresponding silylamines has been achieved simply by heating the silylamine in supercritical carbon dioxide (scCO2), and these O-silylcarbamates have been shown to be effective precursors for the synthesis of a range of symmetrical and unsymmetrical ureas.

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