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. 2008 Oct;34(3):151-3.
doi: 10.1016/j.ssnmr.2008.05.001. Epub 2008 May 27.

Combination of (13)C-(13)C COSY and DARR (COCODARR) in solid-state NMR

Masashi Fukuchi  1 , K Takegoshi
Affiliations

Combination of (13)C-(13)C COSY and DARR (COCODARR) in solid-state NMR

Masashi Fukuchi et al. Solid State Nucl Magn Reson. 2008 Oct.

Abstract

In this work, we describe a new 2D (13)C-(13)C correlation experiment in solids, in which (13)C-(13)C J-correlation (COSY) and dipolar correlation (DARR) are recorded at the same time. The sequence is similar to COCONOSY in the liquid-state NMR, in which (1)H-(1)H COSY and NOESY spectra are obtained in a single experiment. The combined COSY and DARR experiment facilitates assignment of (13)C signals in solids.

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