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. 2009:(53):105-6.
doi: 10.1093/nass/nrp053.

Synthesis of deuterated benzyladenine and its application as a surrogate

Nkaelang Modutlwa  1 , Hiroyuki Tada, Yoshiki Sugahara, Koichi Shiraki, Nobuyuki Hara, Yoshihiro Deyashiki, Takayuki Ando, Tomohiro Maegawa, Yasunari Monguchi, Hironao Sajiki
Affiliations

Synthesis of deuterated benzyladenine and its application as a surrogate

Nkaelang Modutlwa et al. Nucleic Acids Symp Ser (Oxf). 2009.

Abstract

Palladium on carbon-ethylenediamine complex [Pd/C(en)] catalyzed deuteration of N(6)-benzyladenine-d(5), which is a plant growth regulator, to introduce 5 deuterium atoms, while use of Pd/C as a catalyst led to a complete removal of N(6)-benzyl group. The corresponding deuterated N(6)-benzyladenine was successfully used as a surrogate compound for the quantitative analysis of residual benzyladenine in crops using LC/MS/MS.

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