doi: 10.1039/b914468d.
Epub 2009 Sep 23.
Double-quantum 19F-19F dipolar recoupling at ultra-fast magic angle spinning NMR: application to the assignment of 19F NMR spectra of inorganic fluorides
Affiliations
- PMID: 19890524
- DOI: 10.1039/b914468d
Item in Clipboard
Double-quantum 19F-19F dipolar recoupling at ultra-fast magic angle spinning NMR: application to the assignment of 19F NMR spectra of inorganic fluorides
Phys Chem Chem Phys.
.
Abstract
A broadband dipolar recoupling method robust to chemical shift is introduced to observe (19)F-(19)F proximities in fluoroaluminates in high magnetic field and at ultra-fast magic angle spinning (>60 kHz).
Similar articles
-
Homonuclear dipolar recoupling under ultra-fast magic-angle spinning: probing 19F-19F proximities by solid-state NMR.J Magn Reson. 2010 Mar;203(1):113-28. doi: 10.1016/j.jmr.2009.12.009. Epub 2009 Dec 14. J Magn Reson. 2010. PMID: 20044288
-
1H and 19F ultra-fast MAS double-quantum single-quantum NMR correlation experiments using three-spin terms of the dipolar homonuclear Hamiltonian.Phys Chem Chem Phys. 2011 May 7;13(17):8024-30. doi: 10.1039/c0cp02202k. Epub 2011 Mar 28. Phys Chem Chem Phys. 2011. PMID: 21442119
-
A new approach in 1D and 2D 13C high-resolution solid-state NMR spectroscopy of paramagnetic organometallic complexes by very fast magic-angle spinning.J Am Chem Soc. 2003 Mar 26;125(12):3438-9. doi: 10.1021/ja0291742. J Am Chem Soc. 2003. PMID: 12643699
-
Homonuclear dipolar recoupling techniques for structure determination in uniformly 13C-labeled proteins.Solid State Nucl Magn Reson. 2009 Nov;36(3):119-28. doi: 10.1016/j.ssnmr.2009.07.003. Epub 2009 Aug 5. Solid State Nucl Magn Reson. 2009. PMID: 19729285 Review.
-
Dipolar recoupling in MAS spectra of biological solids.Nat Struct Biol. 1998 Jul;5 Suppl:508-12. doi: 10.1038/749. Nat Struct Biol. 1998. PMID: 9665180 Review.
Cited by
-
Optimization of band-selective homonuclear dipolar recoupling in solid-state NMR by a numerical phase search.J Chem Phys. 2019 Apr 21;150(15):154201. doi: 10.1063/1.5092986. J Chem Phys. 2019. PMID: 31005077 Free PMC article.
-
Fast Magic-Angle-Spinning 19F Spin Exchange NMR for Determining Nanometer 19F-19F Distances in Proteins and Pharmaceutical Compounds.J Phys Chem B. 2018 Mar 22;122(11):2900-2911. doi: 10.1021/acs.jpcb.8b00310. Epub 2018 Mar 13. J Phys Chem B. 2018. PMID: 29486126 Free PMC article.
LinkOut - more resources
Full Text Sources
