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. 2010 Nov 5;75(21):7400-3.
doi: 10.1021/jo100971j.

Total synthesis of clathculins A and B

Rebecca C Hoye  1 , Gretchen L Anderson, Susan G Brown, Erica E Schultz
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Total synthesis of clathculins A and B

Rebecca C Hoye et al. J Org Chem. .

Abstract

Clathculins A and B represent a new class of vic-diamine alkaloids containing a PA2 unit as the basic structure. We report the first total syntheses of 1 and 2, which confirm the assigned structure of each. Dependence of their NMR spectroscopic behavior as a function of protonation state has been observed.

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