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. 2008 Jan 9;64(Pt 2):o390.
doi: 10.1107/S1600536807068134.

Morpholinium perchlorate

Mikhail S Grigoriev  1 , Konstantin E German, Alesia Ya Maruk
Affiliations

Morpholinium perchlorate

Mikhail S Grigoriev et al. Acta Crystallogr Sect E Struct Rep Online. .

Abstract

In the title salt, C(4)H(10)NO(+)·ClO(4) (-), which has three independent formula units, the cations are linked into chains along [100] by N-H⋯O hydrogen bonds. Each cation acts both as a donor and as an acceptor, and every cation makes one N-H⋯O hydrogen bond with a ClO(4) (-) anion. The crystal studied was an inversion twin.

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Figures

Fig. 1.
Fig. 1.
A view of (I), showing the atom-labelling scheme. Displacement ellipsoids are drawn at the 50% probability level and H atoms are represented by circles of arbitrary size. Dashed lines indicate the hydrogen-bonding interaction.
Fig. 2.
Fig. 2.
The unit cell of (I).
Fig. 3.
Fig. 3.
The comparison of two different types of chains.
See this image and copyright information in PMC

References

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    1. Flack, H. D. (1983). Acta Cryst. A39, 876–881.
    1. Grigoriev, M. S., German, K. E. & Maruk, A. Y. (2007). Acta Cryst. E63, m2355.
    1. Sheldrick, G. M. (1997a). SHELXS97 and SHELXL97 University of Göttingen, Germany.