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. 2008 Jan 16;64(Pt 2):o463.
doi: 10.1107/S1600536808001190.

5,7-Di-2-pyridyl-2,3-dihydro-thieno[3,4-b][1,4]dioxine

Brandon Djukic, Laura E Harrington, James F Britten, Martin T Lemaire

5,7-Di-2-pyridyl-2,3-dihydro-thieno[3,4-b][1,4]dioxine

Brandon Djukic et al. Acta Crystallogr Sect E Struct Rep Online. .

Abstract

The title compound, C(16)H(12)N(2)O(2)S, was prepared by a Neigishi cross-coupling reaction to investigate the coordination chemistry of thio-phene-containing ligands. In the mol-ecule, the pyridine rings are twisted from the thio-phene ring by 20.6 (1) and 4.1 (2)°. The six-membered dihydro-dioxine ring is in a half-chair conformation.

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Figures

Fig. 1.
Fig. 1.
The molecular structure of the title compound with atom labels and 50% probability displacement ellipsoids for non-H atoms.
See this image and copyright information in PMC

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