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. 2009 Aug 19;65(Pt 9):o2190.
doi: 10.1107/S1600536809031869.

N,N'-Bis(2-thienylmethyl-ene)benzene-1,4-diamine

Affiliations

N,N'-Bis(2-thienylmethyl-ene)benzene-1,4-diamine

Nai-Wei Dong et al. Acta Crystallogr Sect E Struct Rep Online. .

Abstract

The Schiff base, C(16)H(12)N(2)S(2), has been synthesized by refluxing an ethano-lic solution of thio-phene-2-carbaldehyde and benzene-1,4-diamine. The center of the benzene ring is located on a crystallographic center of inversion. The dihedral angle between the benzene and thio-phene rings is 63.6 (1)°.

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Figures

Fig. 1.
Fig. 1.
View of the molecular structure of the title compound, showing the atomic numbering scheme and 50% probability displacement ellipsoids. Atoms labeled with A at the symmetry positions (-x + 1,-y + 1,-z + 1).

References

    1. Andersen, L. H., Nielsen, I. B., Kristensen, M. B., El Ghazaly, M. O. A., Haacke, S., Nielsen, M. B. & Petersen, M. Å ;. (2005). J. Am. Chem. Soc.127, 12347–12350. - PubMed
    1. Boskovic, C., Bircher, R., Tregenna-Piggott, P. L. W., Güdel, H. U., Paulsen, C., Wernsdorfer, W., Barra, A. L., Khatsko, E., Neels, A. & Stoeckli-Evans, H. (2003). J. Am. Chem. Soc.125, 14046–14058. - PubMed
    1. Bruker (2002). APEX2 Bruker AXS Inc., Madison, Wisconsin, USA.
    1. Bruker (2003). SAINT-Plus Bruker AXS Inc., Madison, Wisconsin, USA.
    1. Kannappan, R., Tanase, S., Mutikainen, I., Turpeinen, U. & Reedijk, J. (2005). Inorg. Chim. Acta, 358, 383–388.