Skip to main page content
U.S. flag

An official website of the United States government

Dot gov

The .gov means it’s official.
Federal government websites often end in .gov or .mil. Before sharing sensitive information, make sure you’re on a federal government site.

Https

The site is secure.
The https:// ensures that you are connecting to the official website and that any information you provide is encrypted and transmitted securely.

Access keys NCBI Homepage MyNCBI Homepage Main Content Main Navigation
. 2009 Sep 26;65(Pt 10):o2522-3.
doi: 10.1107/S1600536809037830.

4-(9-Anthr-yl)-1-(3-bromo-phen-yl)spiro-[azetidine-3,9'-xanthen]-2-one

Ismail Celik, Mehmet Akkurt, Aliasghar Jarrahpour, Edris Ebrahimi, Orhan Büyükgüngör

4-(9-Anthr-yl)-1-(3-bromo-phen-yl)spiro-[azetidine-3,9'-xanthen]-2-one

Ismail Celik et al. Acta Crystallogr Sect E Struct Rep Online. .

Abstract

In the title mol-ecule, C(35)H(22)BrNO(2), the four-membered ring of the β-lactam unit is nearly planar [maximum deviation = 0.003 (3) Å] and makes dihedral angles of 87.07 (15), 59.80 (16) and 20.81 (19)°, respectively, with the xanthene system, the anthracene system and the bromo-substituted benzene ring. The mol-ecular conformation is stabilized by weak intra-molecular C-H⋯O and C-H⋯N hydrogen bonds. The crystal structure features weak C-H⋯π inter-actions.

PubMed Disclaimer

Figures

Fig. 1.
Fig. 1.
The title molecular structure, with the atom-numbering scheme and 30% probability displacement ellipsoids
Fig. 2.
Fig. 2.
A view down the a axis of the packing of (I).
See this image and copyright information in PMC

References

    1. Akkurt, M., Jarrahpour, A., Ebrahimi, E., Gençaslan, M. & Büyükgüngör, O. (2008). Acta Cryst. E64, o2466–o2467. - PMC - PubMed
    1. Akkurt, M., Karaca, S., Jarrahpour, A., Ebrahimi, E. & Büyükgüngör, O. (2008). Acta Cryst. E64, o902–o903. - PMC - PubMed
    1. Akkurt, M., Karaca, S., Jarrahpour, A. A., Khalili, D. & Büyükgüngör, O. (2006). Acta Cryst. E62, o866–o868.
    1. Akkurt, M., Yalçın, Ş. P., Jarrahpour, A. A., Nazari, M. & Büyükgüngör, O. (2007). Acta Cryst. E63, o3729–o3730.
    1. Altomare, A., Burla, M. C., Camalli, M., Cascarano, G. L., Giacovazzo, C., Guagliardi, A., Moliterni, A. G. G., Polidori, G. & Spagna, R. (1999). J. Appl. Cryst.32, 115–119.