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. 2009 Dec 12;66(Pt 1):o136.
doi: 10.1107/S1600536809053069.

2-Methyl-5-nitro-benzene-sulfonamide

2-Methyl-5-nitro-benzene-sulfonamide

Muhammad Zia-Ur-Rehman et al. Acta Crystallogr Sect E Struct Rep Online. .

Abstract

In the title compound, C(7)H(8)N(2)O(4)S, the nitro group is twisted by 9.61 (2)° relative to the benzene ring. In the crystal, mol-ecules are linked by N-H⋯O and N-H⋯(O,O) hydrogen bonds between the amino and sulfonyl groups, forming layers parallel to (001).

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Figures

Fig. 1.
Fig. 1.
The molecular structure of (I), with displacement ellipsoids at the 50% probability level.
Fig. 2.
Fig. 2.
Perspective view of the three-dimensional crystal packing showing intermolecular hydrogen-bonded interactions (dashed lines). [Symmetry codes: (i) -x + 1, y + 1/2, -z + 3/2; (ii) x + 1, y, z and (iii) -x + 2, y + 1/2, -z + 3/2]. H atoms not involved in hydrogen bonding have been omitted for clarity.

References

    1. Allen, F. H., Kennard, O., Watson, D. G., Brammer, L., Orpen, A. G. & Taylor, R. (1987). J. Chem. Soc. Perkin Trans 2, pp. S1–19.
    1. Arshad, M. N., Khan, I. U., Zia-ur-Rehman, M. & Shafiq, M. (2009). Acta Cryst. E65, o1204. - PMC - PubMed
    1. Bruker (2007). APEX2 and SAINT Bruker AXS Inc., Madison, Wisconsin, USA.
    1. Farrugia, L. J. (1999). J. Appl. Cryst.32, 837–838.
    1. Flack, H. D. (1983). Acta Cryst. A39, 876–881.