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. 2008 Oct 9;64(Pt 11):o2082.
doi: 10.1107/S1600536808031073.

(S)-N-[(1S,2S)-2-Benzyl-amino-1-(4-hy-droxy-phen-yl)-3-methyl-butyl]-1,1-di-methyl-ethane-2-sulfinamide

Affiliations

(S)-N-[(1S,2S)-2-Benzyl-amino-1-(4-hy-droxy-phen-yl)-3-methyl-butyl]-1,1-di-methyl-ethane-2-sulfinamide

Chun Shen. Acta Crystallogr Sect E Struct Rep Online. .

Abstract

The title compound, C(22)H(32)N(2)O(2)S, was obtained by dehydroxy-lation and deacetyl-ation of 4-{(1S,2S)-2-(benzylhydroxy-amino)-3-methyl-1-[(S)-2-methyl-propane-2-sulfinylamino]but-yl}phenyl acetate, which was derived from reductive crosslinking of nitrone with N-tert-butane-sulfinyl-imine. The crystal structure shows that the mol-ecules are linked by O-H⋯O hydrogen bonds.

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Figures

Fig. 1.
Fig. 1.
Plot of C22H32N2O2S at the 50% probability level. H atoms are drawn as spheres of arbitrary radius.
Fig. 2.
Fig. 2.
Hydrogen bonding in the title compound. Symmetry codes: (i) -x + 1, y + 1/2, -z + 3/2.
Fig. 3.
Fig. 3.
Molecular packing plot, viewed along a axis. Hydrogen bond interactions are shown as dashed lines.

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