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. 2008 Oct 9;64(Pt 11):o2082.
doi: 10.1107/S1600536808031073.

(S)-N-[(1S,2S)-2-Benzyl-amino-1-(4-hy-droxy-phen-yl)-3-methyl-butyl]-1,1-di-methyl-ethane-2-sulfinamide

Chun Shen  1
Affiliations

(S)-N-[(1S,2S)-2-Benzyl-amino-1-(4-hy-droxy-phen-yl)-3-methyl-butyl]-1,1-di-methyl-ethane-2-sulfinamide

Chun Shen. Acta Crystallogr Sect E Struct Rep Online. .

Abstract

The title compound, C(22)H(32)N(2)O(2)S, was obtained by dehydroxy-lation and deacetyl-ation of 4-{(1S,2S)-2-(benzylhydroxy-amino)-3-methyl-1-[(S)-2-methyl-propane-2-sulfinylamino]but-yl}phenyl acetate, which was derived from reductive crosslinking of nitrone with N-tert-butane-sulfinyl-imine. The crystal structure shows that the mol-ecules are linked by O-H⋯O hydrogen bonds.

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Figures

Fig. 1.
Fig. 1.
Plot of C22H32N2O2S at the 50% probability level. H atoms are drawn as spheres of arbitrary radius.
Fig. 2.
Fig. 2.
Hydrogen bonding in the title compound. Symmetry codes: (i) -x + 1, y + 1/2, -z + 3/2.
Fig. 3.
Fig. 3.
Molecular packing plot, viewed along a axis. Hydrogen bond interactions are shown as dashed lines.
See this image and copyright information in PMC

References

    1. Bennai, Y. L. & Hanessian, S. (1997). Chem. Rev.97, 3161–3196. - PubMed
    1. Bruker (2001). SMART, SAINT and SADABS Bruker AXS Inc., Madison, Wisconsin, USA.
    1. Flack, H. D. (1983). Acta Cryst. A39, 876–881.
    1. Kizirian, J. C. (2008). Chem. Rev.108, 140–205. - PubMed
    1. Sheldrick, G. M. (2008). Acta Cryst. A64, 112–122. - PubMed