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. 2009 Jan 14;65(Pt 2):o308.
doi: 10.1107/S1600536809000932.

1-Benzoyl-3-(5-quinol-yl)thio-urea

Wen-Hu Du, Chang-Mei Wei, Wei-Feng Wang

1-Benzoyl-3-(5-quinol-yl)thio-urea

Wen-Hu Du et al. Acta Crystallogr Sect E Struct Rep Online. .

Abstract

The title compound, C(17)H(13)N(3)OS, was obtained by the reaction of benzoyl chloride, ammonium thio-cyanate and 5-amino-quinoline in the presence of polyethyl-eneglycol-400 (PEG-400) as a phase-transfer catalyst. The compound crystallized as discrete mol-ecules linked by N-H⋯N and C-H⋯N hydrogen bonds involving all the potential donors, generating sheets parallel to (100). An intramolecular N-H⋯O bond is also present.

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Figures

Fig. 1.
Fig. 1.
The molecular structure of (I), with atom labels and 50% probability displacement ellipsoids for non-H atoms.
Fig. 2.
Fig. 2.
The packing of (I), viewed down the a axis, showing two layers of molecules connected by van der waals.
See this image and copyright information in PMC

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