Skip to main page content
U.S. flag

An official website of the United States government

Dot gov

The .gov means it’s official.
Federal government websites often end in .gov or .mil. Before sharing sensitive information, make sure you’re on a federal government site.

Https

The site is secure.
The https:// ensures that you are connecting to the official website and that any information you provide is encrypted and transmitted securely.

Access keys NCBI Homepage MyNCBI Homepage Main Content Main Navigation
. 2009 May 14;65(Pt 6):o1267.
doi: 10.1107/S1600536809016778.

1,2-Dibenzoyl-hydrazine-dimethyl-formamide (3/1)

Qing-Peng He, Hong-Gang Li, Guang-Bo Wang, Feng-Lian Fu, Ming-Shi Liu

1,2-Dibenzoyl-hydrazine-dimethyl-formamide (3/1)

Qing-Peng He et al. Acta Crystallogr Sect E Struct Rep Online. .

Abstract

The title compound, 3C(14)H(12)N(2)O(2)·C(3)H(7)NO, was synthesized by reaction of benzoyl chloride with hydrazine hydrate under microwave irradition. The asymmetric unit comprises three 1,2-dibenzoyl-hydrazine mol-ecules and one dimethyl-formamide mol-ecule. The 1,2-dibenzoyl-hydrazine mol-ecules are linked by pairs of N-H⋯O hydrogen bonds into chains propagating along [010].

PubMed Disclaimer

Figures

Fig. 1.
Fig. 1.
The content of asymmetric unit of the title compound showing the atomic numbering scheme and 30% probability displacement ellipsoids.The solvent molecular is omitted for clarity.
See this image and copyright information in PMC

References

    1. Galema, S. A. (1997). Chem. Soc. Rev.26, 233–238.
    1. Shanmuga Sundara Raj, S., Yamin, B. M., Boshaala, A. M. A., Tarafder, M. T. H., Crouse, K. A. & Fun, H.-K. (2000). Acta Cryst. C56, 1011–1012. - PubMed
    1. Sheldrick, G. M. (1996). SADABS University of Göttingen, Germany.
    1. Sheldrick, G. M. (2008). Acta Cryst. A64, 112–122. - PubMed
    1. Siemens (1996). SMART and SAINT Siemens Analytical X-ray Systems, Inc., Madison, Wisconsin, USA.