Skip to main page content
U.S. flag

An official website of the United States government

Dot gov

The .gov means it’s official.
Federal government websites often end in .gov or .mil. Before sharing sensitive information, make sure you’re on a federal government site.

Https

The site is secure.
The https:// ensures that you are connecting to the official website and that any information you provide is encrypted and transmitted securely.

Access keys NCBI Homepage MyNCBI Homepage Main Content Main Navigation
. 2009 Jul 25;65(Pt 8):o1989.
doi: 10.1107/S1600536809027366.

N'-(3,4-Dimethoxy-benzyl-idene)acetohydrazide

N'-(3,4-Dimethoxy-benzyl-idene)acetohydrazide

Lu-Ping Lv et al. Acta Crystallogr Sect E Struct Rep Online. .

Abstract

In the title mol-ecule, C(11)H(14)N(2)O(3), the acetohydrazide group is planar 0.084 (1) Å and forms a dihedral angle of 19.7 (1)° with the benzene ring. One of the meth-oxy groups is coplanar with the attached benzene ring within 0.052 (3) Å, whereas the other is slightly twisted [C-O-C-C = 6.3 (3)°]. The mol-ecule adopts a trans configuration with respect to the C=N bond. In the crystal, the mol-ecules are linked into chains along the a axis by N-H⋯O hydrogen bonds and the chains are cross-linked into a three-dimensional network by C-H⋯O hydrogen bonds.

PubMed Disclaimer

Figures

Fig. 1.
Fig. 1.
The molecular structure of the title compound. Displacement ellipsoids are drawn at the 40% probability level.
Fig. 2.
Fig. 2.
Part of the crystal packing of the title compound. Hydrogen bonds are shown as dashed lines.

References

    1. Bruker (2002). SMART, SAINT and SADABS Bruker AXS Inc., Madison, Wisconsin, USA.
    1. Cimerman, Z., Galic, N. & Bosner, B. (1997). Anal Chim. Acta, 343, 145–153.
    1. Li, Y.-F. & Jian, F.-F. (2008). Acta Cryst. E64, o2409. - PMC - PubMed
    1. Offe, H. A., Siefen, W. & Domagk, G. (1952). Z. Naturforsch. Teil B, 7, 446–447.
    1. Richardson, D., Baker, E., Ponka, P., Wilairat, P., Vitolo, M. L. & Webb, J. (1988). Thalassemia: Pathophysiology and Management, Part B, p. 81. New York: Alan R. Liss Inc.