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. 2010 Jun 16;66(Pt 7):o1660.
doi: 10.1107/S1600536810021781.

4-(8-Eth-oxy-2,3-dihydro-1H-cyclo-penta-[c]quinolin-4-yl)butane-1-peroxol

Jean Fotie, Chris F Fronczek, Kyle A Burns, Frank R Fronczek, Cheryl Bain, D Scott Bohle, Ferdinand P Poudeu

4-(8-Eth-oxy-2,3-dihydro-1H-cyclo-penta-[c]quinolin-4-yl)butane-1-peroxol

Jean Fotie et al. Acta Crystallogr Sect E Struct Rep Online. .

Abstract

In the title mol-ecule, C(18)H(23)NO(3), the hydro-per-oxy-butyl substituent is nearly fully extended, with the four torsion angles in the range 170.23 (10)-178.71 (9)°. The O-O distance in the hydro-peroxide group is 1.4690 (13) Å. This group acts as an inter-molecular hydrogen-bond donor to a quinoline N atom. This results in dimeric units about the respective inversion centers, with graph-set notation R(2) (2)(18).

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Figures

Fig. 1.
Fig. 1.
Ellipsoids at the 50% level, with H atoms having arbitrary radius.
Fig. 2.
Fig. 2.
The hydrogen-bonded dimer, with graph set R22(18).
See this image and copyright information in PMC

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