Skip to main page content
U.S. flag

An official website of the United States government

Dot gov

The .gov means it’s official.
Federal government websites often end in .gov or .mil. Before sharing sensitive information, make sure you’re on a federal government site.

Https

The site is secure.
The https:// ensures that you are connecting to the official website and that any information you provide is encrypted and transmitted securely.

Access keys NCBI Homepage MyNCBI Homepage Main Content Main Navigation
. 2010 Jun 26;66(Pt 7):o1832.
doi: 10.1107/S1600536810024487.

1,3,3-Trimethyl-1,2,3,4-tetra-hydro-pyrido[1,2-a]benzimidazol-1-ol

1,3,3-Trimethyl-1,2,3,4-tetra-hydro-pyrido[1,2-a]benzimidazol-1-ol

Sayed Hasan Mehdi et al. Acta Crystallogr Sect E Struct Rep Online. .

Abstract

In the title compound, C(14)H(18)N(2)O, the benzimidazole grouping is close to planar, with a maximum deviation of 0.042 Å; the six-membered non-aromatic ring adopts an envelope conformation. In the crystal structure, mol-ecules are linked into infinite sheets lying parallel to the bc plane by O-H⋯N and C-H⋯O hydrogen bonds.

PubMed Disclaimer

Figures

Fig. 1.
Fig. 1.
The molecular structure of (I) with 50% probability ellipsoids for non-H atoms.
Fig. 2.
Fig. 2.
The crystal packing of (I), viewed down the b axis, showing the molecules linked into sheets lying parallel to bc. Intermolecular hydrogen bonds are shown as dashed lines.

References

    1. Bruker (2009). APEX2, SAINT and SADABS Bruker AXS Inc., Madison, Wisconsin, USA.
    1. Cosier, J. & Glazer, A. M. (1986). J. Appl. Cryst.19, 105–107.
    1. Cremer, D. & Pople, J. A. (1975). J. Am. Chem. Soc.97, 1354–1358.
    1. Grech, O., Sakellariou, R. & Speziale, V. (1994). J. Heterocycl. Chem.31, 509–511.
    1. Horton, D. A., Bourne, G. T. & Smythe, M. L. (2003). Chem. Rev.103, 893–930. - PubMed