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. 2011 Sep 1;67(Pt 9):o2398.
doi: 10.1107/S1600536811033745. Epub 2011 Aug 27.

2,2'-[(1E)-3-Phenyl-prop-2-ene-1,1-di-yl]bis-(3-hy-droxy-5,5-dimethyl-cyclo-hex-2-en-1-one)

Yu-Lin Zhu  1 , Guo-Lan Xiao, Yan-Fen Chen, Rui-Ting Chen, Ying Zhou
Affiliations

2,2'-[(1E)-3-Phenyl-prop-2-ene-1,1-di-yl]bis-(3-hy-droxy-5,5-dimethyl-cyclo-hex-2-en-1-one)

Yu-Lin Zhu et al. Acta Crystallogr Sect E Struct Rep Online. .

Abstract

In the title mol-ecule, C(25)H(30)O(4), the two cyclo-hexene rings adopt envelope conformations. The two hy-droxy groups are involved in the formation of intra-molecular O-H⋯O hydrogen bonds. In the crystal structure, weak inter-molecular C-H⋯O hydrogen bonds link mol-ecules related by translation along the axis a into chains.

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Figures

Fig. 1.
Fig. 1.
View of (I) showing the atom-labelling scheme. Displacement ellipsoids are drawn at the 50% probability level.
Fig. 2.
Fig. 2.
Palladium(II) chloride catalyzed synthesis of the title compound.
See this image and copyright information in PMC

References

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