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. 2010 May 1;23(5):689854.

New Developments in the Field of Monoliths for Chromatography

Frantisek Svec  1
Affiliations

New Developments in the Field of Monoliths for Chromatography

Frantisek Svec. LC GC Eur. .
No abstract available

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Figures

Figure 1
Figure 1
Isocratic separation of small molecules using hypercrosslinked monolithic capillary column prepared from styrene, chloromethylstyrene, and divinylbenzene. Conditions: Column: 180 × 0.1 mm; Mobile phase: 10% water, 10% tetrahydrofuran, 80% acetonitrile; Flow rate: 0.7 mL/min; Pressure: 27.9 MPa; Peaks: 1 - uracil, 2 - benzene, 3 - toluene, 4 - ethylbenzene, 5 -propylbenzene, 6 - butylbenzene, 7 - amylbenzene (Chromatogram courtesy of Jiri Urban)
Figure 2
Figure 2
SEM of poly(glycidyl methacrylate-co-ethylene dimethacrylate) monolith first reacted with cysteamine and then modified with in situ prepared GNPs. (Photo courtesy of Yan Xu).
Figure 3
Figure 3
SEM micrographs of monolith prepared from polyamide PA6. Reproduced from ref. (24) with permission.
Figure 4
Figure 4
Two-dimensional TLC separation of a mixture of labeled peptides using 50 μm thick monolithic poly(butyl methacrylate-co-ethylene dimethacrylate) layer with a virtual ion exchange channel. (Photo courtesy of Yehua Han).
Figure 5
Figure 5
SEM micrograph of silica-based monolith (Photo courtesy of Merck KGaA)
See this image and copyright information in PMC

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References

    1. Svec F, Tennikova TB, Deyl Z. Monolithic materials: preparation, properties, and applications. Elsevier; Amsterdam: 2003.
    1. Guiochon G. J Chromatogr A. 2007;1168:101–168. - PubMed
    1. Svec F. J Chromatogr A. 2010;1217 in press. - PMC - PubMed
    1. Svec F. Am Lab. 2008;40:13–17.
    1. Svec F. LC-GC America. Jun, 2004.

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