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. 2012 Feb 4;48(11):1671-3.
doi: 10.1039/c2cc16200h. Epub 2011 Dec 21.

Reductive heterocoupling mediated by Cp*2U(2,2'-bpy)

Adil Mohammad  1 , Dennis P Cladis, William P Forrest, Phillip E Fanwick, Suzanne C Bart
Affiliations

Reductive heterocoupling mediated by Cp*2U(2,2'-bpy)

Adil Mohammad et al. Chem Commun (Camb). .

Abstract

Trivalent Cp*(2)U(2,2'-bpy) (2) (Cp* = C(5)Me(5), 2,2'-bpy = 2,2'-bipyridine), which has a monoanionic bipyridine, was treated with p-tolualdehyde (a), furfuraldehyde (b), acetone (c), and benzophenone (d). Reduction of the C[double bond, length as m-dash]O bond followed by radical coupling with bipyridine forms the U(iv) derivatives [Cp*(2)U(2,2'-bpy)(OCRR')] (3a-d).

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