Optimal acidulated phosphate fluoride gel etching time for surface treatment of feldspathic porcelain: on shear bond strength to resin composite

Abstract

Objectives: This in vitro study evaluated the shear bond strength (SBS) of resin composite to feldspathic porcelain after acidulated phosphate fluoride (APF) gel treatment over different periods of time.

Methods: One hundred and fifty-six feldspathic specimens were divided into 12 groups. Group C received no treatment (control group). Groups APF1 through APF10, ten experimental groups, were treated with 1.23% APF gel. Each group obtained 1 to 10 minutes of etching time in 1 minute increments, respectively. Group HF2 was treated with 9.6% hydrofluoric acid (HF) for 2 minutes. All specimens were then bonded to a resin composite cylinder using Adper Scotchbond Multi-purpose (3M ESPE) after silane (Monobond-S, Ivoclar Vivadent AG) application. Specimens were stored at 37ºC for 24 hours before the SBS was performed and were recorded in MPa at fracture. Data were analyzed using one-way ANOVA and Tukey's test (α=.05).

Results: HF etching yielded the highest SBS (18.0 ± 1.5 MPa), which was not significantly different from APF gel etching for 6 to 10 minutes (16.0 ± 2.1 to 17.2 ± 1.6 MPa) (P>.05).

Conclusions: APF gel etching for 6 minutes might be used as an alternative etchant to HF acid for bonding resin composite to silanized feldspathic porcelain.

Keywords: Bond strength; acidulated phosphate fluoride gel; feldspathic porcelain; resin composite.

Figure 1.

Shear bond strength testing.

Figure 2.

SEM results of porcelain specimens (original magnification ×2000). A- Control group, B- through K- Etching with 1.23% APF gel for 1 to 10 minutes, respectively, L- Etching with 9.6% HF acid for 2 minutes.