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. 2012 Jan;68(Pt 1):o1-2.
doi: 10.1107/S1600536811051208. Epub 2011 Dec 3.

5',11'-Dihydro-dispiro-[cyclo-hexane-1,6'-indolo[3,2-b]carbazole-12',1''-cyclo-hexa-ne]

5',11'-Dihydro-dispiro-[cyclo-hexane-1,6'-indolo[3,2-b]carbazole-12',1''-cyclo-hexa-ne]

Ilia A Guzei et al. Acta Crystallogr Sect E Struct Rep Online. 2012 Jan.

Abstract

The title compound, C(28)H(30)N(2), is a symmetrical 2:2 product from the condensation of indole and cyclo-hexa-none. It is the only reported 5,11-dihydro-indolo[3,2-b]carbazole compound in which the spiro atoms are quaternary C atoms. Crystals were grown by vapor diffusion in a three-zone electric furnace. The mol-ecule resides on a crystallographic inversion center. The cyclo-hexyl rings are in a slightly distorted chair conformation, whereas the indole units and the spiro-carbons are coplanar within 0.014 Å.

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Figures

Fig. 1.
Fig. 1.
Molecular structure of (I) (Brandenburg, 1999). Displacement ellipsoids are shown at the 50% probability level and C-bound H atoms are omitted. The compound resides on a crystallographic inversion center. Symmetry transformations used to generate equivalent atoms: (i) -x + 1,-y,-z.

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