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. 2012 Jan;68(Pt 1):o201.
doi: 10.1107/S1600536811053694. Epub 2011 Dec 21.

N-(Pyrrolidin-1-ylcarbothio-yl)benzamide

Aisha A Al-Abbasi, Mohamed Ibrahim Mohamed Tahir, Mohammad B Kassim

N-(Pyrrolidin-1-ylcarbothio-yl)benzamide

Aisha A Al-Abbasi et al. Acta Crystallogr Sect E Struct Rep Online. 2012 Jan.

Abstract

In the title compound, C(12)H(14)N(2)OS, the pyrrolidine ring adopts an envelope conformation with the C atom at the 3-position as the flap and makes a dihedral angle of 65.80 (9)° with the benzene ring. In the crystal, N-H⋯O hydrogen bonds join c-glide related mol-ecules into chains extended along [001] that are further connected into (100) layers via C-H⋯O inter-actions.

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Figures

Fig. 1.
Fig. 1.
The molecular structure of the title compound with displacement ellipsods shown at the 30% probability level.
Fig. 2.
Fig. 2.
The crystal packing of the title compound viewed down the c-axis with intermolecular hydrogen bonds drawn as dashed lines.
See this image and copyright information in PMC

References

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    1. Ngah, N., Kassim, M. B. & Yamin, B. M. (2006). Acta Cryst. E62, o4501–o4502.
    1. Oxford Diffraction (2006). CrysAlis CCD and CrysAlis RED Oxford Diffraction, Abingdon, England.