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. 2012 Feb 1;68(Pt 2):o279.
doi: 10.1107/S1600536811054444. Epub 2012 Jan 7.

4-[(3-Nitro-benzyl-idene)amino]-3-(pyridin-4-yl)-1H-1,2,4-triazole-5(4H)-thione

Tian-Bao Li  1 , Ming-Sheng Yang, Bang-Shao Yin
Affiliations

4-[(3-Nitro-benzyl-idene)amino]-3-(pyridin-4-yl)-1H-1,2,4-triazole-5(4H)-thione

Tian-Bao Li et al. Acta Crystallogr Sect E Struct Rep Online. .

Abstract

In the title compound, C(14)H(10)N(6)O(2)S, the dihedral angle between the pyridine and triazole rings is 3.21 (10)°. The mol-ecule is significantly twisted about the N(t)-N(b) (t = triazole and b = benzyl-idene) bond [C-N(t)-N(b)=C = 151.64 (17)°]. In the crystal, mol-ecules are linked by weak N-H⋯N hydrogen bonds, generating C(8) chains propagating in [10[Formula: see text]].

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Figures

Fig. 1.
Fig. 1.
The molecular structure of (I). Displacement ellipsoids are drawn at the 30% probability level.
Fig. 2.
Fig. 2.
The crystal packing for (I).
See this image and copyright information in PMC

References

    1. Liu, X. H., Tan, C. X. & Jian, Q. W. (2011). Phosphorus Sulfur Silicon Relat. Elem. 186, 558–564.
    1. Rigaku/MSC (2005). CrystalClear Rigaku/MSC Inc. The Woodlands, Texas, USA.
    1. Sheldrick, G. M. (2008). Acta Cryst. A64, 112–122. - PubMed
    1. Wang, B. L., Shi, Y. X., Ma, Y., Liu, X. H., Li, Y. H., Song, H. B., Li, B. J. & Li, Z. M. (2010). J. Agric. Food Chem. 58, 5515–5520. - PubMed