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. 2012 Apr 23;51(17):4144-7.
doi: 10.1002/anie.201200961. Epub 2012 Mar 16.

Visible-light photoredox catalysis in flow

Joseph W Tucker  1 , Yuan Zhang, Timothy F Jamison, Corey R J Stephenson
Affiliations

Visible-light photoredox catalysis in flow

Joseph W Tucker et al. Angew Chem Int Ed Engl. .
No abstract available

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Figures

Figure 1
Figure 1
Photoredox Catalysis in Flow: Enabling Increased Efficiency by Reactor Technology.
Figure 2
Figure 2
Oxidation of tetrahydroisoquinolines in flow.
Figure 3
Figure 3
Intramolecular radical reactions in flow.
Figure 4
Figure 4
Intermolecular radical reactions in flow.
Figure 5
Figure 5
Intermolecular ATRA reactions in flow.
See this image and copyright information in PMC

References

    1. For recent reviews of photoredox catalysis in synthetic applications, see: Zeitler K. Angew. Chem. 2009;121:9969. Angew. Chem., Int. Ed. 2009;48:9785. Yoon TP, Ischay MA, Du J. Nature Chem. 2010;2:527. Narayanam JMR, Stephenson CRJ. Chem. Soc. Rev. 2010;40:102. Teplý F. Collect. Czech. Chem. Commun. 2011;76:859. Tucker JW, Stephenson CRJ. J. Org. Chem. 2012;77:1617.

    1. For recent examples from the MacMillan lab, see: Nicewicz DA, MacMillan DWC. Science. 2008;322:77. Nagib DA, Scott ME, MacMillan DWC. J. Am. Chem. Soc. 2009;131:10875. Shih H-W, Vander Wal MN, Grange RL, MacMillan DWC. J. Am. Chem. Soc. 2010;132:13600. Pham PV, Nagib DA, MacMillan DWC. Angew. Chem., Int. Ed. 2011;50:6119. McNally A, Prier CK, MacMillan DWC. Science. 2011;334:1114. Nagib DA, MacMillan DWC. Nature. 2011;480:224.

    1. For recent examples from the Yoon lab, see: Ischay MA, Anzovino ME, Du J, Yoon TP. J. Am. Chem. Soc. 2008;130:12886. Du J, Yoon TP. J. Am. Chem. Soc. 2009;131:14604. Ischay MA, Lu Z, Yoon TP. J. Am. Chem. Soc. 2010;132:8572. Lu Z, Shen M, Yoon TP. J. Am. Chem. Soc. 2011;133:1162. Hurtley AE, Cismesia MA, Ischay MA, Yoon TP. Tetrahedron. 2011;67:4442. Du J, Espelt L. Ruiz, Guzei IA, Yoon TP. Chem. Sci. 2011;2:2115. Lin S, Ischay MA, Fry CG, Yoon TP. J. Am. Chem. Soc. 2011;133:19350.

    1. For selected recent examples of photoredox catalysis in organic synthesis, see: Andrews RS, Becker JJ, Gagné MR. Angew. Chem., Int. Ed. 2010;49:7274. Zou Y-Q, Lu L-Q, Fu L, Chang N-J, Rong J, Chen J-R, Xiao W-J. Angew. Chem., Int. Ed. 2011;50:7171. Rueping M, Leonori D, Poisson T. Chem. Commun. 2011;47:9615. Kalyani D, McMurtrey KB, Neufeldt SR, Sanford MS. J. Am. Chem. Soc. 2011;133:18566. Maity S, Zhu M, Shinabery RS, Zheng N. Angew. Chem., Int. Ed. 2012;51:222.

    1. For selected reviews on organic synthesis conducted in flow, see: Jas G, Kirschning A. Chem. Eur. J. 2003;9:5708. Wiles C, Watts P. Eur. J. Org. Chem. 2008:1655. Webb D, Jamison TF. Chem. Sci. 2010;1:675.

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