Skip to main page content
U.S. flag

An official website of the United States government

Dot gov

The .gov means it’s official.
Federal government websites often end in .gov or .mil. Before sharing sensitive information, make sure you’re on a federal government site.

Https

The site is secure.
The https:// ensures that you are connecting to the official website and that any information you provide is encrypted and transmitted securely.

Access keys NCBI Homepage MyNCBI Homepage Main Content Main Navigation
. 2012 Jul 1;68(Pt 7):o2252.
doi: 10.1107/S1600536812028450. Epub 2012 Jun 30.

(S)-(-)-2-(1H-Indol-3-yl)-N-(1-phenyl-eth-yl)acetamide

Johana Ramírez  1 , Oscar Romero, Jorge R Juárez, Joel L Terán, Angel Mendoza
Affiliations

(S)-(-)-2-(1H-Indol-3-yl)-N-(1-phenyl-eth-yl)acetamide

Johana Ramírez et al. Acta Crystallogr Sect E Struct Rep Online. .

Abstract

In the title compound, C(18)H(18)N(2)O, the dihedral angle between the indole system and the phenyl ring is 17.2 (2)°. The crystal packing features two N-H⋯O hydrogen bonds, which link the mol-ecules into layers parallel to (001). The absolute configuration was determined by the synthetic procedure and was set according to the starting material.

PubMed Disclaimer

Figures

Fig. 1.
Fig. 1.
The molecular structure of title compound, with atom labels and 30% probability displacement ellipsoids for non-H atoms.
Fig. 2.
Fig. 2.
Molecular packing of title compound, viewed down the a axis, showing hydrogen bonds and intramolecular interaction (dashed lines).
See this image and copyright information in PMC

References

    1. Chiou, W.-H., Lin, G.-H., Hsu, C.-C., Chaterpaul, S. & Ojima, I. (2009). Org. Lett. 11, 2659–2662. - PubMed
    1. Farrugia, L. J. (1997). J. Appl. Cryst. 30, 565.
    1. Kochanowska-Karamyan, A. J. & Hamann, M. T. (2010). Chem. Rev. 110, 4489–4497. - PMC - PubMed
    1. North, A. C. T., Phillips, D. C. & Mathews, F. S. (1968). Acta Cryst. A24, 351–359.
    1. Sheldrick, G. M. (2008). Acta Cryst. A64, 112–122. - PubMed