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. 2012 Oct 19;14(20):5342-5.
doi: 10.1021/ol302525m. Epub 2012 Oct 3.

Copper-catalyzed aminooxygenation of N-allylamidines with PhI(OAc)2

Stephen Sanjaya  1 , Shunsuke Chiba
Affiliations

Copper-catalyzed aminooxygenation of N-allylamidines with PhI(OAc)2

Stephen Sanjaya et al. Org Lett. .

Abstract

A Cu-catalyzed aminoacetoxylation of N-alkenylamidines has been achieved using PhI(OAc)(2) as an oxygen source for synthesis of 4-acetoxymethyl-4,5-dihydroimidazoles, which could be further converted into 2,3-diaminopropanol derivatives using AlH(3) as a reductant.

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