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. 2013 Mar 9;69(Pt 4):o508.
doi: 10.1107/S1600536813005862. Print 2013 Apr 1.

5-Iodo-3-phenyl-2,1-benzoxazole

Yuriy Teslenko  1 , Vasyl S Matiychuk, Vasyl Kinzhybalo, Tadeusz Lis, Mykola D Obushak
Affiliations

5-Iodo-3-phenyl-2,1-benzoxazole

Yuriy Teslenko et al. Acta Crystallogr Sect E Struct Rep Online. .

Abstract

The title compound, C13H8INO, was prepared by a condensation reaction of 4-nitro-benzene with phenyl-acetonitrile in NaOH-ethanol solution. There are two independent mol-ecules in the asymmetric unit, in which the dihedral angles between the benzene ring and the benzoisoxazole unit are 4.2 (3) and 4.1 (3)°. The crystal packing is governed by C-H⋯N, C-I⋯π and C-I⋯O inter-actions.

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Figures

Fig. 1.
Fig. 1.
The asymmetric unit of the title compound with atom labeling scheme. The displacement ellipsoids are drawn at the 50% probability level.
Fig. 2.
Fig. 2.
The crystal packing of the title compound showing intermolecular interactions as dashed lines (molecule A - red, molecule B - green).
See this image and copyright information in PMC

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