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. 2013 Jul-Aug;37(6):321-5.
doi: 10.1093/jat/bkt036. Epub 2013 May 10.

An HPLC-HR-MS-MS method for identification of anticoagulant rodenticides in blood

Jason E Schaff  1 , Madeline A Montgomery
Affiliations

An HPLC-HR-MS-MS method for identification of anticoagulant rodenticides in blood

Jason E Schaff et al. J Anal Toxicol. 2013 Jul-Aug.

Abstract

This paper presents a fully validated method for the qualitative identification of bromadiolone, brodifacoum, coumachlor, coumatetralyl, difenacoum and warfarin in whole blood specimens. Samples are protein precipitated with acetonitrile, processed via solid-phase extraction and analyzed by high-performance liquid chromatography with high resolution tandem mass spectrometric detection. Limits of detection were 10 ng/mL or better for all analytes.

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