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. 2013 Sep 18;69(Pt 10):o1549.
doi: 10.1107/S1600536813025075. eCollection 2013.

4-{(E)-[2-(Pyridin-3-ylcarbon-yl)hydrazinyl-idene]meth-yl}phenyl acetate

Riya Datta  1 , V Ramya, M Sithambaresan, M R Prathapachandra Kurup
Affiliations

4-{(E)-[2-(Pyridin-3-ylcarbon-yl)hydrazinyl-idene]meth-yl}phenyl acetate

Riya Datta et al. Acta Crystallogr Sect E Struct Rep Online. .

Abstract

The title compound, C15H13N3O3, exists in the E conformation with respect to the azo-methane C=N double bond. The pyridyl and phenyl rings form dihedral angles of 35.67 (8) and 36.65 (7)°, respectively with the central C(=O)N2C unit. In the crystal, N-H⋯O and C-H⋯O hydrogen bonds connect the mol-ecules into chains along the b axis. Another C-H⋯O inter-action connects mol-ecules along the c-axis direction, forming layers.

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Figures

Fig. 1.
Fig. 1.
ORTEP view of the title compound drawn with 50% probability displacement ellipsoids for the non-H atoms.
Fig. 2.
Fig. 2.
Hydrogen-bonding interactions in the crystal structure of C15H13N3O3.
Fig. 3.
Fig. 3.
π···π interactions in the crystal structure of C15H13N3O3.
Fig. 4.
Fig. 4.
Packing diagram of the compound along the b axis.
See this image and copyright information in PMC

References

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