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. 2013 Sep 18;69(Pt 10):o1551-2.
doi: 10.1107/S1600536813025336. eCollection 2013.

(3aR,6S,7aR)-7a-Chloro-2-[(4-nitro-phen-yl)sulfon-yl]-1,2,3,6,7,7a-hexa-hydro-3a,6-ep-oxy-iso-indole

Ersin Temel  1 , Aydın Demircan, Muhammet Kasım Kandemir, Medine Colak, Orhan Büyükgüngör
Affiliations

(3aR,6S,7aR)-7a-Chloro-2-[(4-nitro-phen-yl)sulfon-yl]-1,2,3,6,7,7a-hexa-hydro-3a,6-ep-oxy-iso-indole

Ersin Temel et al. Acta Crystallogr Sect E Struct Rep Online. .

Abstract

In the title compound, C14H13ClN2O5S, the chlorine-substituted tetrahydrofuran ring adopts a twist conformation and the other tetra-hydro-furan ring an envelope conformation with the O atom as the flap. The pyrrolidine ring adopts a twist conformation. In the crystal, C-H⋯O hydrogen bonds link the mol-ecules into zigzag chains running along the b-axis direction.

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Figures

Fig. 1.
Fig. 1.
Synthesis of the title compound.
Fig. 2.
Fig. 2.
The molecular structure of the title compound, with displacement ellipsoids drawn at the 30% probability level.
Fig. 3.
Fig. 3.
Part of the crystal structure of the title compound, showing the formation of R22(10) rings.
See this image and copyright information in PMC

References

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