Skip to main page content
U.S. flag

An official website of the United States government

Dot gov

The .gov means it’s official.
Federal government websites often end in .gov or .mil. Before sharing sensitive information, make sure you’re on a federal government site.

Https

The site is secure.
The https:// ensures that you are connecting to the official website and that any information you provide is encrypted and transmitted securely.

Access keys NCBI Homepage MyNCBI Homepage Main Content Main Navigation
. 2013 Sep 21;69(Pt 10):o1576.
doi: 10.1107/S1600536813025749. eCollection 2013.

(E)-N-(1,3-Benzodioxol-5-yl)-1-(4-{[1-(prop-2-en-1-yl)-1H-1,2,3-triazol-4-yl]meth-oxy}phen-yl)methanimine

Mehmet Akkurt  1 , Aliasghar Jarrahpour, Mehdi Mohammadi Chermahini, Pezhman Shiri, Orhan Büyükgüngör
Affiliations

(E)-N-(1,3-Benzodioxol-5-yl)-1-(4-{[1-(prop-2-en-1-yl)-1H-1,2,3-triazol-4-yl]meth-oxy}phen-yl)methanimine

Mehmet Akkurt et al. Acta Crystallogr Sect E Struct Rep Online. .

Abstract

In the title compound, C20H18N4O3, the dihedral angles between the central benzene ring and the 1H-1,2,3-triazole ring and the fused benzene ring are 65.34 (19) and 3.64 (18)°, respectively. The dioxole ring adopts a shallow envelope conformation, with the methyl-ene C atom displaced by 0.156 (5) Å from the other four atoms (r.m.s. deviation = 0.007Å). In the crystal, the mol-ecules are linked by C-H⋯O and C-H⋯N hydrogen bonds, generating a three-dimensional network.

PubMed Disclaimer

Figures

Fig. 1.
Fig. 1.
The molecular structure of compound (I) with 30% probability displacement ellipsoids.
Fig. 2.
Fig. 2.
Packing diagram of compound (I) viewed down the a axis. Hydrogen bonds are indicated by broken lines. H atoms not participating in hydrogen bonding have been omitted for clarity.
Fig. 3.
Fig. 3.
A packing diagram for compound (I), viewed down the c axis, showing the hydrogen-bonding network. H atoms not participating in hydrogen bonding have been omitted for clarity.
See this image and copyright information in PMC

References

    1. Arora, K., Gupta, A. & Agarwal, D. D. (2002). Asian J. Chem. 14, 1611–1615.
    1. Calligaris, M. & Randaccio, L. (1987). Comprehensive Coordination Chemistry, Vol. 2, p 715. Oxford: Pergamon.
    1. Farrugia, L. J. (2012). J. Appl. Cryst. 45, 849–854.
    1. Macho, V., Kralik, M., Hudec, J. & Cingelova, J. (2004). J. Mol. Catal. A Chem. 209, 69–73.
    1. Sheldrick, G. M. (2008). Acta Cryst. A64, 112–122. - PubMed