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. 2014 Mar 12;70(Pt 4):o418.
doi: 10.1107/S1600536814004929. eCollection 2014 Apr 1.

(Z)-3-[2-(2,4-Di-nitro-phen-yl)hydrazin-1-yl-idene]isobenzo-furan-1(3H)-one di-chloro-methane hemisolvate

Palak Agarwal  1 , Pragati Mishra  1 , Nikita Gupta  1 , Neelam  1 , Priyaranjan Sahoo  1 , Satish Kumar  1
Affiliations

(Z)-3-[2-(2,4-Di-nitro-phen-yl)hydrazin-1-yl-idene]isobenzo-furan-1(3H)-one di-chloro-methane hemisolvate

Palak Agarwal et al. Acta Crystallogr Sect E Struct Rep Online. .

Abstract

In the title compound, 2C14H8N4O6·CH2Cl2, the di-chloro-methane solvent mol-ecule resides on a crystallographic twofold axis. The mean plane of the phthaliso-imide ring is oriented at a dihedral angle of 32.93 (12)° with respect to the nitro-substituted benzene ring. An intra-molecular N-H⋯O hydrogen bond occurs. The crystal packing features a short Cl⋯O halogen-bond inter-action [3.093 (3) Å].

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Figures

Fig. 1.
Fig. 1.
The molecular structure of the title compound, with atom labels and 50% probability displacement ellipsoids for non-H atoms.
Fig. 2.
Fig. 2.
The packing diagram of the title compound viewed viewed along b axis, showing short intermolecular O···Cl halogen bonds and intramolecular N—H···O hydrogen bonds.
See this image and copyright information in PMC

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