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. 2014 Apr 5;70(Pt 5):o515.
doi: 10.1107/S1600536814007028. eCollection 2014 May 1.

1-{[(Z)-Cyclo-pentyl-idene]amino}-3-phenyl-thio-urea

Joel T Mague  1 , Shaaban K Mohamed  2 , Mehmet Akkurt  3 , Alaa A Hassan  4 , Mustafa R Albayati  5
Affiliations

1-{[(Z)-Cyclo-pentyl-idene]amino}-3-phenyl-thio-urea

Joel T Mague et al. Acta Crystallogr Sect E Struct Rep Online. .

Abstract

The sample of the title compound, C12H15N3S, chosen for study consisted of triclinic crystals twinned by a 180° rotation about the a axis. The five-membered ring adopts a twisted conformation. The dihedral angle between the phenyl ring and the mean plane of the thio-urea unit is 78.22 (8)°. In the crystal, molecules are linked via pairs of N-H⋯S hydrogen bonds forming inversion dimers.

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Figures

Fig. 1.
Fig. 1.
Perspective view of I with 50% probability displacement ellipsoids.
Fig. 2.
Fig. 2.
Packing viewed down the a axis and showing N—H···S interactions.
See this image and copyright information in PMC

References

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