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. 2014 Apr 26;70(Pt 5):o613.
doi: 10.1107/S160053681400912X. eCollection 2014 May 1.

N-(2-Nitro-phen-yl)thio-phene-2-carbox-amide

Rodolfo Moreno-Fuquen  1 , Alexis Azcárate  1 , Alan R Kennedy  2
Affiliations

N-(2-Nitro-phen-yl)thio-phene-2-carbox-amide

Rodolfo Moreno-Fuquen et al. Acta Crystallogr Sect E Struct Rep Online. .

Abstract

The title compound, C11H8N2O3S, shows two mol-ecules per asymmetric unit, with the dihedral angles between the benzene and thio-phene rings of 13.53 (6) and 8.50 (5)° being a notable difference between them. An intra-molecular N-H⋯O hydrogen-bond in each mol-ecule generates an S(6) ring motif. The crystal packing shows no classical hydrogen bonds with the mol-ecules being packed to form weak C-H⋯O and C-H⋯S inter-actions leading to R 2 (2)(9) and R 4 (4)(25) rings which are edge-shared, giving layers parallel to (010).

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Figures

Fig. 1.
Fig. 1.
Molecular conformation and atom numbering scheme for the title compound with displacement ellipsoids drawn at the 50% probability level. H atoms are shown as spheres of arbitrary radius.
Fig. 2.
Fig. 2.
Part of the crystal structure of (I), showing the formation of edge-fused R22(9) and R44(25) rings running parallel to (010).
See this image and copyright information in PMC

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