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. 2016 Jun 27;55(27):7742-6.
doi: 10.1002/anie.201601445. Epub 2016 May 30.

The Preparation of Complexes of Germanone from a Germanium μ-Oxo Dimer

Soumen Sinhababu  1 , Dhirendra Yadav  1 , Surendar Karwasara  1 , Mahendra Kumar Sharma  1 , Goutam Mukherjee  1 , Gopalan Rajaraman  2 , Selvarajan Nagendran  3
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The Preparation of Complexes of Germanone from a Germanium μ-Oxo Dimer

Soumen Sinhababu et al. Angew Chem Int Ed Engl. .

Abstract

Complexes of germanone containing formal Ge=O→M bonds (M=Zn, B, Ge, Sn) were isolated and characterized. The compounds were prepared through a novel synthetic route using a germanium μ-oxo dimer 3 as the starting material. This method circumvents the need to employ germanones to prepare complexes of germanones.

Keywords: Lewis acids; NMR spectroscopy; germanium; germanone; structure elucidation.

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