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. 2016 Sep:78:37-39.
doi: 10.1016/j.ssnmr.2016.06.003. Epub 2016 Jun 27.

High-temperature MAS-NMR at high spinning speeds

Holger Kirchhain  1 , Julian Holzinger  1 , Adrian Mainka  1 , Andreas Spörhase  1 , Sabarinathan Venkatachalam  1 , Achim Wixforth  1 , Leo van Wüllen  1
Affiliations

High-temperature MAS-NMR at high spinning speeds

Holger Kirchhain et al. Solid State Nucl Magn Reson. 2016 Sep.

Abstract

A low cost version to enable high temperature MAS NMR experiments at temperatures of up to 700°C and spinning speeds of up to 10kHz is presented. The method relies on inductive heating using a metal coated rotor insert. The metal coating is accomplished via a two step process involving physical vapor deposition and galvanization.

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