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. 2020 Oct-Dec;10(4):435-440.
doi: 10.1016/j.jobcr.2020.07.006. Epub 2020 Aug 5.

Effect of fluoride agents on surface characteristics of NiTi wires. An ex vivo investigation

Prasad Chitra  1 , G S Prashantha  2 , Arun Rao  3
Affiliations

Effect of fluoride agents on surface characteristics of NiTi wires. An ex vivo investigation

Prasad Chitra et al. J Oral Biol Craniofac Res. 2020 Oct-Dec.

Abstract

Aim: To analyze the degree of corrosion of nickel titanium arch wires in patients with and without exposure to fluorides.

Material and methods: This was an ex vivo study comprising of 60 subjects undergoing fixed orthodontic treatment. Group 1(controls) comprised of 30 sets of new unused NiTi wires and unused 11, 15 brackets, Group 2(patients) comprised of 30 sets of non fluoridated NiTi wires and 11, 15 brackets and Group 3(patients) had 30 sets of fluoridated NiTi wires and 11, 15 brackets. NiTi wires were used over 6 months of treatment(0.014″,0.016″, 16 × 22", each wire was used for 2 months and replaced with the next size). All wires were retrieved, stored and analyzed. At 6 months, brackets from 11 to 15 were debonded in both treatment groups. Archwires and brackets in 3 groups were subjected to SEM analysis at 500 and 1000X to observe differences. Additionally, EDX Spectroscopy was undertaken to evaluate surface elemental compositional differences in groups.

Results: Significant differences among groups were evident in brackets and archwires tested. Maximum degradation, cracks and dark spots were seen in wires and brackets exposed to fluoride agents. EDX spectroscopy revealed least Ni% in fluoridated wires and brackets.

Conclusions: Increased leaching of metal ions was evident when wires and brackets are exposed to fluoride agents during treatment. Use of non fluoridated mouthwash and toothpastes may be considered in orthodontic patients without risk of caries to mitigate such effects.

Keywords: Corrosion; EDX Spectroscopy; Fluoride; NiTi; SEM.

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Conflict of interest statement

Nil.

Figures

Fig. 1
Fig. 1
SEM surface morphology of a) unused, b) non fluoridated & c) fluoridated 0.014″ NiTi.
Fig. 2
Fig. 2
SEM surface morphology of a) unused, b) non fluoridated & c) fluoridated 0.016″ NiTi.
Fig. 3
Fig. 3
SEM surface morphology of a) unused, b)non fluoridated & c) fluoridated 16 × 22″ NiTi.
Fig. 4
Fig. 4
SEM surface morphology of a) unused, b) non fluoridated & c) fluoridated incisor bracket.
Fig. 5
Fig. 5
SEM surface morphology of a) unused, b)non fluoridated & c)fluoridated premolar.
Fig. 6
Fig. 6
EDX Spectroscopy elemental analysis of 0.014″ NiTi wires used in the study. Maximal %.
See this image and copyright information in PMC

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