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. 2020 Sep 18;5(Pt 9):x201248.
doi: 10.1107/S2414314620012481. eCollection 2020 Sep.

2,2'-Oxybis[1,3-bis-(4-meth-oxy-phen-yl)-2,3-di-hydro-1 H-benzo[ d][1,3,2]di-aza-borole]

Hannah H Mallard  1 , Nicholas D Kennedy  1 , Nathan A Rudman  2 , Alexa M Greenwood  1 , Jonathan Nicoleau  1 , Corey E Angle  1 , Nicole A Torquato  3 , Michael R Gau  2 , Patrick J Carroll  2 , Mitchell R Anstey  1
Affiliations

2,2'-Oxybis[1,3-bis-(4-meth-oxy-phen-yl)-2,3-di-hydro-1 H-benzo[ d][1,3,2]di-aza-borole]

Hannah H Mallard et al. IUCrdata. .

Abstract

In the title compound, C40H36B2N4O5, the B-O-B bond angle is 132.75 (13) and the dihedral angle between the benzodiazborole rings is 73.02 (5)°. In the crystal, weak C-H⋯O inter-actions link the mol-ecules.

Keywords: boron; bridging μ-oxo; crystal structure.

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Figures

Figure 1
Figure 1
The mol­ecular structure of the title compound. Hydrogen atoms have been omitted for clarity. Ellipsoids are at 50% probability.
Figure 2
Figure 2
Chemical scheme for the synthesis of the title compound.
See this image and copyright information in PMC

References

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