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. 2022 Oct 29;15(21):7616.
doi: 10.3390/ma15217616.

Effect of Polyphenylene Sulphide Particles and Films on the Properties of Polyphenylene Sulphide Composites

Zeyu Sun  1   2 , Li Sun  3 , Chengyan Zhu  1   2 , Wei Tian  1   2 , Lingda Shao  1 , Xuhuang Feng  1 , Kunzhen Huang  1
Affiliations

Effect of Polyphenylene Sulphide Particles and Films on the Properties of Polyphenylene Sulphide Composites

Zeyu Sun et al. Materials (Basel). .

Abstract

Glass fibre-reinforced polyphenylene sulphide composites were prepared by hot-pressing glass fibre fabrics and polyphenylene sulphide resins. The effects of different polyphenylene sulphide resin forms on the properties of the composites were investigated using scanning electron microscopy, dynamic mechanical analyser, pendulum impact tester and universal testing machine. The results showed that different polyphenylene sulphide resin forms had nearly no effect on the glass transition temperature of the composites, which are all located at about 100 °C. Compared with other polyphenylene sulphide composites, the bending strength of polyphenylene sulphide film composites was the highest, reaching 314.58 MPa, and the impact strength of polyphenylene sulphide particle composites was the highest, reaching 245.4 KJ/m2. The bending strength and impact strength were calculated using a standard fraction, and the highest standard fraction was obtained when the ratio of polyphenylene sulphide film to particle was 1:2. The impact strength and bending strength could be obtained. The impact strength reached 229.8 KJ/m2, and the bending strength reached 284.16 MPa.

Keywords: composite laminate; dynamic mechanical analysis; flexural properties; glass fibre; impact properties; polyphenylene sulphide.

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Conflict of interest statement

The authors declare no conflict of interest.

Figures

Figure 1
Figure 1
Glass fibre modification.
Figure 2
Figure 2
(a) Digieye top view shot of PPS film; (b) Digieye top view shot of PPS particles.
Figure 3
Figure 3
Composite laminate structure diagram. (a) P0F6, pure PPS film; (b) P2F4, the ratio of film to particle is 2:1; (c) P4F2, the ratio of film to particle is 1:2; (d) P6F0, pure PPS particles.
Figure 4
Figure 4
Hot pressing diagram. 1, upper cover plate; 2, polyimide film; 3, prefabricated parts; 4, polyimide film; 5, filler piece; 6, lower mould.
Figure 5
Figure 5
(a) Testing bending performance with the universal testing machine; (b) pendulum impact tester testing impact performance.
Figure 6
Figure 6
IR spectra of PPS in different forms.
Figure 7
Figure 7
Effect of different polyphenylene sulphide forms on the dynamic mechanical properties of composites: (a) storage modulus; (b) loss modulus.
Figure 7
Figure 7
Effect of different polyphenylene sulphide forms on the dynamic mechanical properties of composites: (a) storage modulus; (b) loss modulus.
Figure 8
Figure 8
Effect of PPS form on mechanical properties of composites.
Figure 9
Figure 9
SEM cross-sectional image of impact fracture pattern of Glass Fibre Fabric Reinforced PPS Composite (a) PPS (particle) and glass fibre tow; (b) PPS (film) and glass fibre tow; (c) combination of film and particle.
See this image and copyright information in PMC

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