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. 2023 Apr 13;59(31):4648-4651.
doi: 10.1039/d3cc00259d.

Chiral carbonyl hypoiodites

Milla Mattila  1 , Kari Rissanen  1 , Jas S Ward  1
Affiliations

Chiral carbonyl hypoiodites

Milla Mattila et al. Chem Commun (Camb). .

Abstract

Three chiral carbonyl hypoiodites, R-C(O)OI, have been prepared from N-protected (S)-valine to give the ligand-stabilised (S)-valinoyl hypoiodite complexes with 4-dimethylaminopyridine, 4-pyrrolidinopyridine, and 4-morpholinopyridine as the stabilising ligands. The identity of the complexes was established by NMR (1H, 13C, 1H-15N HMBC) and single crystal X-ray diffraction analysis.

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